University of Mumbai

Class: S.E. Branch:Instrumentation Semester: IV
Subject: Analytical Instrumentation (Abbreviated as AI)
Periods per Week(60 min. each)

Lecture

04
Practical 02
Tutorial
Hours Marks
Evaluation System

Theory

3 100
Practical/Oral

Oral

25

Term Work

25

Total

3 150

 

 

all syllabus in single     PDF file free download . SEM IV INST

Module

Contents

Hours
1 Overview & IntroductionIntroduction  to  the  analytical  processes  &  ElectromagneticSpectrum. 02
2 Basics of SpectroscopyLaws of photometry- Light and its interaction with matterIntroduction to Spectroscopic MethodsComponents of  Optical Systems  (viz.  Radiation sources & detectors,   filters  &  monochromators,  signal  processors  & readouts.) 05
3 Atomic SpectroscopyAtomic absorption spectroscopyAtomic Emission Spectroscopy 05
4 Molecular SpectroscopyElectronic TransitionsIntroduction to UV-Visible molecular spectroscopyApplications of UV-Visible spectroscopy

Fluorescence, phosphorescence and chemiluminescence’s

Raman scattering & Raman spectrophotometer

Nuclear Transitions

Nuclear Magnetic Resonance (NMR)

Vibrational Excitation

IR absorption spectroscopy

Applications of Infrared Spectrometry

14
5 Additional Instrumental Methods for Organic StructuralAnalysisMass Spectrometry 03
6 Separation ScienceFundamentals of chromatographic separationsGas chromatography- Gas chromatograph & its componentsHigh performance liquid chromatography 06

 

 

7 Industrial Gas AnalyzersOxygen,  Carbon  dioxide,  and  NOx  analyzers,  Online  GasAnalyzers.Nephalometer, Densitometer, 05
8 Radio Chemical InstrumentationRadio   Chemical   methods,   radiation   detectors-   ionizationchamber,    Giger-Muller      counter,     proportional      counter, scintillation  counter,  semiconductor  detectors,  pulse  height analyzer,    X-ray     spectrometry,     X-ray     spectrum,     X-ray spectrometry, X-ray diffractometers, X-ray absorption meter. 05

 

 

 

Theory Examination:

1.         Question paper will consist of total 7 questions, of 20 marks each.

2.         Only 5 questions need to be attempted.

3.         Q.1 will be compulsory covering entire syllabus.

4.         Remaining questions will be of mixed nature.

5.         In  question  paper  weightage  of  each  module  will  be  proportional  to  the number of respective lecture hours as mentioned in the syllabus.

 

 

 

 

Practical/Oral Examination:

Practical  examination  will  be  based  on  one  experiment  performed  from  the  list  of

experiments given in the syllabus and the oral will be based on entire subject.

 

Term work:

Term work consists of minimum eight experiments and a written test. The distribution of

the term work marks shall be as follows,

Laboratory work (Experiments and Journal)                          :10 marks Test (at least one)                                                                                                :10 marks Attendance (Practical and Theory)                                                                            :05 marks

The final certification and acceptance of term-work ensures the satisfactory performance of laboratory work and minimum passing in the term-work.

 

 

 

List of Laboratory Experiments:

1.  Photoelectric Colorimeter

2.  Nephalo-turbidity meter

3.  Densitometer

4.  Refractometer

5.  Single beam Spectrometer for UV/VIS range.

6.  Double beam Spectrometer for UV/VIS range.

7.  Gas Chromatograph

8.  Atomic absorption spectrometer

9.  Balance Cell Calorimeter

10. Spectroflourimeter

 

Books Recommended:

 

1.  Skoog, Holler, Nieman, Thomson Principles of Instrumental Analysis, Books-cole publications, 5th ed..

2.  Willard, Merritt, Dean, Settle, Instrumental Methods of Analysis, CBS Publishers

& Distributors, New Delhi, 7th ed..

3.  Khandpur  R.  S.,  Handbook  of  Analytical  Instruments,  Tata  McGraw–Hill

Publications, 3rd ed..

4.  Ewing  Galen  W.,  Instrumental  Methods  of  Chemical  Analysis,  McGraw-Hill

Book Company, 5th ed..

5.  Braun  Robert  D.,  Introduction  to  Instrumental  Analysis,  McGraw-Hill  Book

Company.

6.  Sherman R.E., Analytical Instrumentation, ISA Publication.

 

all syllabus in single     PDF file free download . SEM IV INST